1: With naphthalene; lithium in tetrahydrofuran T=-15°C; Ring cleavage; metalation; 7 h; 2: With water in tetrahydrofuran Substitution; reduction; 0.25 h; Title compound not separated from byproducts;
lithium aluminium tetrahydride in tetrahydrofuran 144 h; Heating;
参考文献
Wijsman, Geerlig W.; Van Der Veen, Lars A.; De Wolf, Willem H.; Bickelhaupt, Friedrich
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 10 p. 2095 - 2098