反应条件
1: 43 percent / 1.) mol. sieves 4 Angstroem, 2.) Me3Si-OTf / CH2Cl2 / 1.) -10 deg C, 10 min, 2.) a.) -10 deg C, 15 min, b.) 0 deg C, 15 min 2: 76 percent / H2 / Pd/C / ethyl acetate; methanol / 1 h / 760 Torr / Ambient temperature View Scheme
参考文献
Rathore, Hargovind; From, Arthur H. L.; Ahmed, Khalil; Fullerton, Dwight S.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 10 p. 1945 - 1952
