(4E)-4-癸烯-1-醇合成路线 （共 18 条）
反应条件
1: 84 percent / n-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide 2: LiAlH4 / tetrahydrofuran; bis-(2-methoxy-ethyl) ether / 140 °C 3: p-toluenesulfonic acid / H2O; methanol View Scheme
参考文献
Griepink, Frans C.; Van Beek, Teris A.; Posthumus, Maarten A.; De Groot, Aede; Visser, J. Hans; Voerman, Simon
Tetrahedron Letters, 1996 , vol. 37, # 3 p. 411 - 414
反应条件
1: 84 percent / n-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide 2: LiAlH4 / tetrahydrofuran; bis-(2-methoxy-ethyl) ether / 140 °C 3: p-toluenesulfonic acid / H2O; methanol View Scheme
参考文献
Bestmann; Koschatzky; Schaetzke; et al.
1981 , vol. No. 9, p. 1705 - 1720
反应条件
1: LiAlH4 / tetrahydrofuran; bis-(2-methoxy-ethyl) ether / 140 °C 2: p-toluenesulfonic acid / H2O; methanol View Scheme
参考文献
Griepink, Frans C.; Van Beek, Teris A.; Posthumus, Maarten A.; De Groot, Aede; Visser, J. Hans; Voerman, Simon
Tetrahedron Letters, 1996 , vol. 37, # 3 p. 411 - 414
反应条件
1: 1) Mg / 2) 1 h, heating; 3) 12 h 2: 60 percent / Na / diethyl ether / 12 h View Scheme
参考文献
Bestmann; Koschatzky; Schaetzke; et al.
1981 , vol. No. 9, p. 1705 - 1720
反应条件
diisobutylaluminium hydride in toluene Inert atmosphere; optical yield given as percent de;
参考文献
Cosgrove, Kelly L.; McGeary, Ross P.
Synlett, 2009 , # 11 p. 1749 - 1752
反应条件
zirconocene dichloride; oxygen; diisobutyl-aluminum chloride 1.) 20 deg C, 2 h, 2.) hexane, 4 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Dzhemilev, U. M.; Ibragimov, A. G.; Vostrikova, O. S.; Vasil'eva, E. V.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, p. 1004 - 1009
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , vol. 36, # 5 p. 1089 - 1095
反应条件
diisobutylaluminium hydride reaction with phosphorane prepared different way; Product distribution;
参考文献
Boland, Wilhelm; Ney, Peter; Jaenicke, Lothar
Synthesis, 1980 , # 12 p. 1015 - 1017
反应条件
pyridinium chlorochromate in dichloromethane 2 h;
参考文献
Bestmann; Koschatzky; Schaetzke; et al.
1981 , vol. No. 9, p. 1705 - 1720
