1-(2-甲基丙基)-4-硝基苯合成路线 (共 10 条)
反应条件
nitric acid; acetic anhydride 2 h; Ambient temperature;
参考文献
Hartmann; Batzl
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 5 p. 537 - 544
反应条件
nitric acid in dichloromethane 24 h; Ambient temperaturefurther monosubstituted benzenes; variuos conditions; Product distributionMechanism;
参考文献
Strazzolini, Paolo; Giumanini, Angelo G.; Runcio, Antonio; Scuccato, Massimo
Journal of Organic Chemistry, 1998 , vol. 63, # 4 p. 952 - 958
反应条件
triphenylphosphine; [(CO)4Fe(μ-PPh2)Pd(μ-Cl)]2 in benzene T=78°C; 20 h;
参考文献
Shenglof, Margarita; Gelman, Dmitri; Heymer, Bernd; Schumann, Herbert; Molander, Gary A.; Blum, Jochanan
Synthesis, 2003 , # 2 p. 302 - 306
反应条件
copper(II) nitrate; K10 clay in acetic anhydride 2 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Laszlo, Pierre; Vandormael, Joseph
Chemistry Letters, 1988 , p. 1843 - 1846
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=55 - 60°C; 4 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Jacobs, Bruce D.; Kwon, Soon-Jae; Field, Leslie D.; Norris, Robert K.; Randles, David; et al.
Tetrahedron Letters, 1985 , vol. 26, # 29 p. 3495 - 3498
反应条件
sulfuric acid; nitric acid T=0 - 3°C;
参考文献
Salesskaja
Zhurnal Obshchei Khimii, 1947 , vol. 17, p. 489,494
Chem.Abstr., 1948 , p. 844
反应条件
1: red phosphorus; iodine; aqueous HI 2: concentrated H2SO4; aqueous HNO3 / 0 - 3 °C View Scheme
参考文献
Salesskaja
Zhurnal Obshchei Khimii, 1947 , vol. 17, p. 489,494
Chem.Abstr., 1948 , p. 844
参考文献
Salesskaja
Zhurnal Obshchei Khimii, 1947 , vol. 17, p. 489,494
Chem.Abstr., 1948 , p. 844
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Hartmann; Batzl
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 5 p. 537 - 544
参考文献
Salesskaja
Zhurnal Obshchei Khimii, 1947 , vol. 17, p. 489,494
Chem.Abstr., 1948 , p. 844