in acetone under inert gas; dropwise addn. of p-MeOC6H4NC in acetone to a suspn. of the Pt complex in the presence of NaBF4 at room temp.; stirring for 1 h; solvent removed, residue dissolved in CH2Cl2; soln. filtered and concd., addn. of Et2O yields the solid;
参考文献
Michelin, Rino A.; Zanotto, Livio; Braga, Dario; Sabatino, Piera; Angelici, Robert J.
Inorganic Chemistry, 1988 , vol. 27, p. 85 - 92
in acetone under inert gas; dropwise addn. of the isocyanide in acetone to the suspn. of the Pd complex in acetone in presence of NaBF4 at room temp.; stirring for 1 h; solvent removed, residue dissolved in CH2Cl2; soln. filtered and concd., addn. of Et2O yields the solid; elem. anal.;
参考文献
Michelin, Rino A.; Zanotto, Livio; Braga, Dario; Sabatino, Piera; Angelici, Robert J.
Inorganic Chemistry, 1988 , vol. 27, p. 85 - 92
in acetone under inert gas; dropwise addn. of the isocyanide in acetone to a suspn. of the Pt complex in acetone in the presence of NaBF4 at room temp.; vigorous stirring for 1 h; solvent removed, residue dissolved in CH2Cl2; soln. filtrated, concd. to a small vol.; addn. of Et2O yields the solid; elem. anal.;
参考文献
Michelin, Rino A.; Zanotto, Livio; Braga, Dario; Sabatino, Piera; Angelici, Robert J.
Inorganic Chemistry, 1988 , vol. 27, p. 85 - 92
in acetone under inert gas; dropwise addn. of the isocyanide in acetone to the suspn. of the Pd complex in acetone in presence of NaBF4 at room temp.; stirring for 1 h; solvent removed, residue dissolved in CH2Cl2; soln. filtered and concd., addn. of Et2O yields the solid; elem. anal.;
参考文献
Michelin, Rino A.; Zanotto, Livio; Braga, Dario; Sabatino, Piera; Angelici, Robert J.
Inorganic Chemistry, 1988 , vol. 27, p. 85 - 92
