3-氰基-5-甲氧基苯硼酸频那醇酯合成路线 （共 3 条）
反应条件
potassium acetate; tri-cyclo-hexyl-phosphine; tris-(dibenzylideneacetone)dipalladium(0) in ethylene glycol dimethyl ether T=150°C; 1 h; Irradiation in a microwave;
参考文献
ASTRAZENECA AB; ASTEX THERAPEUTICS LTD
Patent: WO2008/76046 A1, 2008 ;
Location in patent: Page/Page column 117-118 ;
WO 2008/076046 A1
反应条件
bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I); 4,4'-di-tert-butyl-2,2'-dipyridyl in tert-butyl methyl ether T=80°C; 18 h; Inert atmosphere;
参考文献
Zeqing, Li; Zhibin, Liang; Yuqiang, Wang; Pei, Yu
Research on Chemical Intermediates, 2013 , vol. 39, # 4 p. 1917 - 1926
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; 2,6-di-tert-butyl-pyridine T=130°C; Microwave irradiation;
参考文献
Xiao, Dong; Palani, Anandan; Sofolarides, Michael; Huang, Ying; Aslanian, Robert; Vaccaro, Henry; Hong, Liwu; McKittrick, Brian; West Jr., Robert E.; Williams, Shirley M.; Wu, Ren-Long; Hwa, Joyce; Sondey, Christopher; Lachowicz, Jean
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 2 p. 861 - 864
