1: in diethyl ether
T=0°C; Grignard reaction; Inert atmosphereCooling with ice;
2: With water; ammonium chloride in diethyl ether
Grignard reaction; Inert atmosphere;
参考文献
Palmer, Cory; Morra, Nicholas A.; Stevens, Andrew C.; Bajtos, Barbora; Machin, Ben P.; Pagenkopf, Brian L.
Organic Letters, 2009 , vol. 11, # 24 p. 5614 - 5617