1,3,5-环庚三烯-1-甲酰氯合成路线 （共 3 条）
反应条件
1: 56 percent / Br2, aq. NaOH / dioxane / 2.5 h / 0 - 20 °C 2: thionyl chloride, pyridine / 1 h / Heating View Scheme
参考文献
Higuchi, Hiroyuki; Kondo, Masao; Yonehara, Hiroko; Ojima, Juro; Iyoda, Masahiko
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 1 p. 275 - 281
反应条件
pyridine; thionyl chloride 1 h; Heating;
参考文献
Higuchi, Hiroyuki; Kondo, Masao; Yonehara, Hiroko; Ojima, Juro; Iyoda, Masahiko
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 1 p. 275 - 281
反应条件
1: benzene / 0.5 h / Heating
2: 85 percent / LiAlH4 / tetrahydrofuran; diethyl ether / 1 h / Ambient temperature
3: 64 percent / BaMnO4 / CH2Cl2 / 23 h / Ambient temperature
View Scheme
参考文献
Higuchi, Hiroyuki; Kondo, Masao; Yonehara, Hiroko; Ojima, Juro; Iyoda, Masahiko
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 1 p. 275 - 281
