(R)-1-苯基-1,3-丙二醇合成路线 (共 39 条)
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=20°C; 1 h;
参考文献
Xu, Chengfu; Yuan, Chengye
Tetrahedron, 2005 , vol. 61, # 8 p. 2169 - 2186
反应条件
1: With thionyl chloride in methanol T=0°C; 1 h; 2: With sodium tetrahydroborate in methanol 0.5 h;
参考文献
Khatik, Gopal L.; Sharma, Ratnesh; Kumar, Varun; Chouhan, Mangilal; Nair, Vipin A.
Tetrahedron Letters, 2013 , vol. 54, # 45 p. 5991 - 5993
反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride in ethylene glycol dimethyl ether; toluene 3 h; Ambient temperature;
参考文献
Gao, Y.; Sharpless, K. B.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4081 - 4084
反应条件
1: With oxygen; ozone in pentane T=-78°C; 1 h; 2: With lithium aluminium tetrahydride in tetrahydrofuran; pentane T=65°C; 1 h;
参考文献
Denmark, Scott E.; Beutner, Gregory L.; Wynn, Thomas; Eastgate, Martin D.
Journal of the American Chemical Society, 2005 , vol. 127, # 11 p. 3774 - 3789
反应条件
1: With ozone 2: With lithium aluminium tetrahydride
参考文献
Denmark, Scott E.; Heemstra Jr., John R.
Journal of Organic Chemistry, 2007 , vol. 72, # 15 p. 5668 - 5688
反应条件
lithium aluminium tetrahydride in tetrahydrofuran; diethyl ether T=0°C; 0.5 h;
参考文献
Organic Letters, , vol. 9, # 19 p. 3793 - 3796
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; Reduction;
参考文献
Corey; Choi, Soongyu
Tetrahedron Letters, 2000 , vol. 41, # 16 p. 2769 - 2772
反应条件
1: With ozone 2: With lithium aluminium tetrahydride
参考文献
Denmark, Scott E.; Heemstra Jr., John R.
Journal of Organic Chemistry, 2007 , vol. 72, # 15 p. 5668 - 5688
反应条件
1: With oxygen; ozone in dichloromethane T=-78°C; 0.333333 h; 2: With lithium aluminium tetrahydride in tetrahydrofuran; dichloromethane T=65°C; 1.5 h; Further stages.;
参考文献
Denmark, Scott E.; Heemstra Jr., John R.
Journal of Organic Chemistry, 2007 , vol. 72, # 15 p. 5668 - 5688
反应条件
sodium tetrahydroborate in methanol Yield given;
参考文献
Tetrahedron Letters, , vol. 37, # 51 p. 9253 - 9254