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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
10355-12-1
合成路线
（共 77 条）
128796-39-4
4-三氟甲基苯硼酸
+
459-64-3
4-甲氧苯重氮四氟硼酸盐
→
反应条件
10355-12-1
反应条件
(IMes)Pd(NQ) in ethanol T=50°C; Suzuki Coupling; 1 h; Conversion of starting material;
参考文献
Karch, Ralf; Briel, Oliver; Kayser, Bernd; Beller, Matthias; Selvakumar, Kumaravel; Frisch, Anja; Zapf, Alexander
Patent: US2006/122398 A1, 2006 ;
Location in patent: Page/Page column 8-9 ;
5720-07-0
4-甲氧基苯硼酸
+
98-56-6
对氯三氟甲苯
→
反应条件
10355-12-1
反应条件
K3PO4*3H2O; (2-mesityl-1H-inden-3-yl)dicyclohexylphosphine; palladium diacetate; Aliquatreg; 336 in water T=20 - 100°C; Suzuki-Miyaura Coupling; 8 h; Inert atmosphere;
参考文献
Mao, Shu-Lan; Sun, Yue; Yu, Guang-Ao; Zhao, Cui; Han, Zhi-Jun; Yuan, Jia; Zhu, Xiaolei; Yang, Qihua; Liu, Sheng-Hua
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 47 p. 9410 - 9417
402-43-7
对溴三氟甲苯
+
130952-94-2
→
反应条件
10355-12-1
反应条件
potassium fluoride; palladium diacetate; tris-(o-tolyl)phosphine in N,N-dimethyl-formamide T=120°C;
参考文献
Hatanaka, Yasuo; Goda, Ken-ichi; Okahara, Yoshinori; Hiyama, Tamejiro
Tetrahedron, 1994 , vol. 50, # 28 p. 8301 - 8316
98-56-6
对氯三氟甲苯
+
13139-86-1
3-甲基-CBS-氧硼啶
→
反应条件
10355-12-1
反应条件
C20H23BrN4Ni in tetrahydrofuran T=25°C; Kumada Cross-Coupling; 24 h; Inert atmosphere;
参考文献
Sun, Yunqiang; Li, Xiaoyan; Sun, Hongjian
Dalton Transactions, 2014 , vol. 43, # 25 p. 9410 - 9413
3899-91-0
→
反应条件
10355-12-1
反应条件
potassium hydroxide; palladium diacetate in methanol T=60°C; Suzuki-Miyaura cross-coupling;
参考文献
Zhang, Liang; Meng, Tianhao; Wu, Jie
Journal of Organic Chemistry, 2007 , vol. 72, # 24 p. 9346 - 9349
402-43-7
对溴三氟甲苯
+
33397-21-6
→
反应条件
10355-12-1
+
2132-80-1
4,4-二甲氧基联苯
反应条件
caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl acetamide T=90°C; 2 h;
参考文献
Rao, Maddali L.N.; Jadhav, Deepak N.; Banerjee, Debasis
Tetrahedron, 2008 , vol. 64, # 24 p. 5762 - 5772
623-12-1
4-氯苯甲醚
+
128796-39-4
4-三氟甲基苯硼酸
→
反应条件
10355-12-1
反应条件
potassium fluoride; bis(benzonitrile)palladium(II) dichloride in tetrahydrofuran T=25°C; Suzuki-Miyaura Coupling; 16 h; Inert atmosphereSealed tube;
参考文献
Iwai, Tomohiro; Tanaka, Ryotaro; Harada, Tomoya; Sawamura, Masaya
Chemistry - A European Journal, 2014 , vol. 20, # 4 p. 1057 - 1065
104-92-7
4-溴苯甲醚
+
214360-65-3
4-(三氟甲基)苯硼酸频哪醇酯
→
反应条件
10355-12-1
反应条件
potassium phosphate; (C5H5FeC5H3C(CH3)NC6H4CH3)PdCl(tricyclohexylphosphine); potassium acetate in 1,4-dioxane; water T=100°C; Suzuki coupling; 3 h; Inert atmosphere;
参考文献
Wang, Lianhui; Cui, Xiuling; Li, Jingya; Wu, Yusheng; Zhu, Zhiwu; Wu, Yangjie
European Journal of Organic Chemistry, 2012 , # 3 p. 595 - 603
402-43-7
对溴三氟甲苯
+
171364-79-7
4-甲氧基苯硼酸频那醇酯
→
反应条件
10355-12-1
反应条件
potassium phosphate; (C5H5FeC5H3C(CH3)NC6H4CH3)PdCl(tricyclohexylphosphine); potassium acetate in 1,4-dioxane; water T=100°C; Suzuki coupling; 3 h; Inert atmosphere;
参考文献
Wang, Lianhui; Cui, Xiuling; Li, Jingya; Wu, Yusheng; Zhu, Zhiwu; Wu, Yangjie
European Journal of Organic Chemistry, 2012 , # 3 p. 595 - 603
455-13-0
4-碘三氟甲苯
+
213596-33-9
→
反应条件
10355-12-1
反应条件
copper(l) iodide; (o-tBu2P-C6H4)NMe2; cesium fluoride in 1,4-dioxane; N,N-dimethyl-formamide T=120°C; Suzuki-Miyaura Coupling; 48 h; GloveboxInert atmosphere;
参考文献
Gurung, Santosh K.; Thapa, Surendra; Kafle, Arjun; Dickie, Diane A.; Giri, Ramesh
Organic Letters, 2014 , vol. 16, # 4 p. 1264 - 1267
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