反应条件
ammonia; EDTA; HCl in ethanol; water High Pressure; to a soln. of metal salt with EDTA at pH 2-3 (HCl, NH3) added a water/ethanol soln. of NH4F, treated at 180°C for 20 h; cooled to room temp., ppt. filtered, washed (water), dried (80°C,air); XRD, TEM;
参考文献
Liang, Xin; Wang, Xun; Wang, Leyu; Yan, Ruoxue; Peng, Qing; Li, Yadong
European Journal of Inorganic Chemistry, 2006 , # 11 p. 2186 - 2191
