in dichloromethane Addn. of Fe-complex soln. to a suspn. of the Co-complex under N2, stirring (0.5 h).; Evapn. to dryness, column chromy. (Florisil, hexane) gives Co- and mixed Co-Fe-complexes and as the last fraction the Co5Fe-complex, recryst. (CH2Cl2/hexane), elem. anal.. Further products.;

in dichloromethane under Ar, Fe-complex dropwise added, soln. stirred (4 h, room temp.); evapn., extn. (Et2O);

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in tetrahydrofuran byproducts: C6H6; Irradiation (UV/VIS); irradn. for 38 h; monitored by IR;