[R-(Z)]-4-羟基-N,N,N-三甲基-9-氧代-7-[(三苯基甲氧基)甲基]-3,5,8-三氧杂-4-磷杂二十六碳-17-烯-1-铵内盐 4-氧化物合成路线 （共 6 条）
反应条件
sodium in dimethyl sulfoxide T=20°C; 0.5 h;
参考文献
Wang, Pingzhen; Blank, David H.; Spencer, Thomas A.
Journal of Organic Chemistry, 2004 , vol. 69, # 8 p. 2693 - 2702
反应条件
1: 67 percent / ZnCl2 / dimethylformamide / 10 h / 5 °C 2: 81 percent / sodium / dimethylsulfoxide / 0.5 h / 20 °C View Scheme
参考文献
Borsotti, Gianpietro; Guglielmetti, Gianfranco; Spera, Silvia; Battistel, Ezio
Tetrahedron, 2001 , vol. 57, # 51 p. 10219 - 10227
反应条件
1: tetrahydrofuran / 0.75 h / 20 °C 2: 81 percent / sodium / dimethylsulfoxide / 0.5 h / 20 °C View Scheme
参考文献
Borsotti, Gianpietro; Guglielmetti, Gianfranco; Spera, Silvia; Battistel, Ezio
Tetrahedron, 2001 , vol. 57, # 51 p. 10219 - 10227
反应条件
1: 67 percent / ZnCl2 / dimethylformamide / 10 h / 5 °C 2: 81 percent / sodium / dimethylsulfoxide / 0.5 h / 20 °C View Scheme
参考文献
Borsotti, Gianpietro; Guglielmetti, Gianfranco; Spera, Silvia; Battistel, Ezio
Tetrahedron, 2001 , vol. 57, # 51 p. 10219 - 10227
反应条件
boron trifluoride-diethyl ether complex; sodium hydrogencarbonate in methanol; dichloromethane; water
参考文献
CL Pharma Aktiengesellschaft
Patent: US4814112 A1, 1989 ;
反应条件
boron trifluoride diethyl etherate; O-MEM-ricinoleic acid anhydride in dichloromethane T=0°C; 1 h;
参考文献
Borsotti, Gianpietro; Guglielmetti, Gianfranco; Spera, Silvia; Battistel, Ezio
Tetrahedron, 2001 , vol. 57, # 51 p. 10219 - 10227
