S-(4-甲基苯基)苯硫代甲酸酯合成路线 (共 63 条)
反应条件
1: hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; oxygen; 1,2-bis-(diphenylphosphino)ethane / chlorobenzene / 9 h / Air atmosphere; Reflux
2: hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; triphenylphosphine; 1,2-bis-(diphenylphosphino)ethane / tetrahydrofuran / 5 h / Inert atmosphere; Reflux
View Scheme
参考文献
Arisawa, Mieko; Igarashi, Yui; Kobayashi, Haruki; Yamada, Toru; Bando, Kentaro; Ichikawa, Takuya; Yamaguchi, Masahiko
Tetrahedron, 2011 , vol. 67, # 40 p. 7846 - 7859
反应条件
sodium hydroxide in dimethyl sulfoxide
参考文献
Appleyard,G.D.; Stirling,C.J.M.
Journal of the Chemical Society [Section] C: Organic, 1967 , p. 2686 - 2691
反应条件
P2O5; 1H-imidazole
1) 50 deg C, 1 h, 2) 80 deg C, 10 h; Yield given. Multistep reaction;
参考文献
Rao, C. Someswara; Rambabu, M.; Srinivasan, P. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 407 - 411
反应条件
T=500°C; P=0.001 - 0.1 Torr; Further byproducts given;
参考文献
Aitken, R. Alan; Drysdale, Martin J.; Ryan, Bruce M.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 20 p. 3345 - 3348
反应条件
1: alcohol; diethyl ether
2: sulfuric acid
View Scheme
参考文献
Chapman
Journal of the Chemical Society, 1926 , p. 2298
反应条件
1: alcohol; diethyl ether
2: sulfuric acid
View Scheme
参考文献
Chapman
Journal of the Chemical Society, 1926 , p. 2298
参考文献
Morgenstern,J.; Mayer,R.
Zeitschrift fuer Chemie (Stuttgart, Germany), 1969 , vol. 9, p. 182 - 183
反应条件
in acetone
T=20°C; 20 h; Product distribution;
参考文献
Churkina, T. D.; Petrova, R. G.; Kandror, I. I.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1946 - 1949
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 9 p. 2130 - 2134
参考文献
Perumal, Subbu; Vasuki, Gnanasambandam; Vijayabaskar, Veerappan; Selvaraj, Sangavanaicker; Boykin, David W.
Magnetic Resonance in Chemistry, 1998 , vol. 36, # 10 p. 720 - 726
参考文献
Gilman; Smith; Parker
Journal of the American Chemical Society, 1925 , vol. 47, p. 858