5-(羟基甲基)二氢呋喃-2(3H)-酮合成路线 （共 15 条）
反应条件
hydrogenchloride; dihydrogen peroxide in methanol; formic acid
参考文献
Nguyen-Ba; Nghe; Quimpere; Miguel; Kong; Laval Chan Chung; Brown; William L.; Dionne; Gervais
Patent: US5789394 A1, 1998 ;
反应条件
V-501 in water T=75°C; 16 h;
参考文献
Yorimitsu, Hideki; Wakabayashi, Katsuyu; Shinokubo, Hiroshi; Oshima, Koichiro
Tetrahedron Letters, 1999 , vol. 40, # 3 p. 519 - 522
Title/Abstract Full Text View citing articles Show Details
Yorimitsu; Wakabayashi; Shinokubo; Oshima
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 10 p. 1963 - 1970
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in 2,2,2-trifluoroethanol T=-20°C;
参考文献
Tellitu, Imanol; Urrejola, Andrea; Serna, Sonia; Moreno, Isabel; Herrero, M. Teresa; Dominguez, Esther; SanMartin, Raul; Correa, Arkaitz
European Journal of Organic Chemistry, 2007 , # 3 p. 437 - 444
反应条件
V-501 in water T=75°C; 16 h;
参考文献
Yorimitsu; Wakabayashi; Shinokubo; Oshima
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 10 p. 1963 - 1970
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in 2,2,2-trifluoroethanol T=-20°C;
参考文献
Tellitu, Imanol; Urrejola, Andrea; Serna, Sonia; Moreno, Isabel; Herrero, M. Teresa; Dominguez, Esther; SanMartin, Raul; Correa, Arkaitz
European Journal of Organic Chemistry, 2007 , # 3 p. 437 - 444
反应条件
titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-DIPT in dichloromethane; toluene T=-20°C; 6 h;
参考文献
Lopp, Margus; Paju, Anne; Kanger, Tonis; Pehk, Tonis
Tetrahedron Letters, 1996 , vol. 37, # 42 p. 7583 - 7586
反应条件
2,2'-azo-bisisobutyronitrile in benzene 8 h; Heating;
参考文献
Kraus, George A.; Landgrebe, Kevin
Tetrahedron Letters, 1984 , vol. 25, # 36 p. 3939 - 3942
Title/Abstract Full Text View citing articles Show Details
Kraus, George A.; Landgrebe, Kevin
Tetrahedron, 1985 , vol. 41, # 19 p. 4039 - 4046
反应条件
sodium tetrahydroborate in methanol T=-30 - -15°C;
参考文献
Journal of Medicinal Chemistry, , vol. 40, # 2 p. 168 - 180
反应条件
1: H2, AcONa / 10percent Pd/C / tetrahydrofuran / 24 h / Ambient temperature 2: 10percent aq. HCl / tetrahydrofuran / 2 h / Ambient temperature 3: NaBH4 / methanol / -30 - -15 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 40, # 2 p. 168 - 180
反应条件
potassium permanganate; water; copper(II) sulfate in dichloromethane 6 h;
参考文献
Baskaran, Sundarababu; Islam, Imadul; Vankar, Padma S.; Chandrasekaran, Srinivasan
Journal of the Chemical Society, Chemical Communications, 1992 , # 8 p. 626 - 627
