反应条件
Multi-step reaction with 3 steps 1: 1.) acetic acid, NaNO2 / 1.) H2O, 0 deg C, 2.) 22 deg C, 18 h2: 1.) phenylselenyl chloride, 2.) H2O2 / 1.) ethyl acetate, 23 deg C, 3 h, 2.) 1 h3: 100 percent / LiAlH4 / diethyl ether; tetrahydrofuran / 0.75 h / 0 °C
参考文献
Avery, Mitchell A.; Tanabe, Masato; Crowe, David F.; Detre, George; Peters, Richard H.; Chong, Wesley K. M. Steroids, 1990 , vol. 55, # 2 p. 59 - 64
