反应条件
1: palladium diacetate; N-bromosuccinmide; 2,2,2-trimethylacetic acid / toluene / 18 h / 100 °C / |Inert atmosphere; |Sealed tube; |Schlenk technique
2: N,N-dimethyl-formamide / 12 h / 120 °C / |Inert atmosphere; |Schlenk technique
3: sodium hydroxide; water / ethanol / 6 h / |Inert atmosphere; |Schlenk technique; |Reflux
View Scheme
参考文献
Tian, Qingshan; Chen, Xianmin; Liu, Wei; Wang, Zechao; Shi, Suping; Kuang, Chunxiang
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 45 p. 7830 - 7833
