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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
103797-32-6
合成路线
（共 8 条）
130198-71-9
→
反应条件
103797-32-6
反应条件
sodium hydroxide in tetrahydrofuran; water 2 h; Reflux;
参考文献
Zhang, Xuan; Bao, Bin; Yu, Xiuhua; Tong, Linjiang; Luo, Yu; Huang, Qingqing; Su, Mingbo; Sheng, Li; Li, Jia; Zhu, Hong; Yang, Bo; Zhang, Xiongwen; Chen, Yi; Lu, Wei
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 22 p. 6981 - 6995
5454-83-1
5-溴戊酸甲酯
→
反应条件
103797-32-6
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 90 °C 2: sodium hydroxide / water; tetrahydrofuran / 2 h / |Reflux View Scheme
参考文献
Zhang, Xuan; Bao, Bin; Yu, Xiuhua; Tong, Linjiang; Luo, Yu; Huang, Qingqing; Su, Mingbo; Sheng, Li; Li, Jia; Zhu, Hong; Yang, Bo; Zhang, Xiongwen; Chen, Yi; Lu, Wei
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 22 p. 6981 - 6995
2067-33-6
5-溴戊酸
→
反应条件
103797-32-6
反应条件
1: thionyl chloride / 2 h / 20 °C 2: potassium carbonate / N,N-dimethyl-formamide / 16 h / 90 °C 3: sodium hydroxide / water; tetrahydrofuran / 2 h / |Reflux View Scheme
参考文献
Zhang, Xuan; Bao, Bin; Yu, Xiuhua; Tong, Linjiang; Luo, Yu; Huang, Qingqing; Su, Mingbo; Sheng, Li; Li, Jia; Zhu, Hong; Yang, Bo; Zhang, Xiongwen; Chen, Yi; Lu, Wei
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 22 p. 6981 - 6995
100-02-7
对硝基苯酚
→
反应条件
103797-32-6
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 90 °C 2: sodium hydroxide / water; tetrahydrofuran / 2 h / |Reflux View Scheme
参考文献
Zhang, Xuan; Bao, Bin; Yu, Xiuhua; Tong, Linjiang; Luo, Yu; Huang, Qingqing; Su, Mingbo; Sheng, Li; Li, Jia; Zhu, Hong; Yang, Bo; Zhang, Xiongwen; Chen, Yi; Lu, Wei
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 22 p. 6981 - 6995
55502-03-9
1-(4-溴丁氧基)-4-硝基苯
→
反应条件
103797-32-6
反应条件
1: potassium cyanide; aqueous ethanol 2: aq.-ethanolic NaOH-solution View Scheme
参考文献
Ashley et al.
Journal of the Chemical Society, 1959 , p. 897,901
28341-54-0
→
反应条件
103797-32-6
反应条件
1: tetrahydrofurfuryl alcohol 2: acetic acid; aqueous hydrochloric acid View Scheme
参考文献
Gerecs; Windholz
Acta Chimica Academiae Scientiarum Hungaricae, 1958 , vol. 14, p. 417,418
13094-50-3
1-(3-溴丙氧基)-4-硝基苯
+
94-02-0
苯甲酰乙酸乙酯
→
反应条件
103797-32-6
反应条件
(i) NaOEt, EtOH, (ii) aq. KOH, MeOH; Multistep reaction;
参考文献
Collins,R.F.; Davis,M.
Journal of the Chemical Society, 1961 , p. 1863 - 1879
103797-32-6
→
反应条件
103852-82-0
5-(4-氨基苯氧基)戊酸
反应条件
Hydrogenation;
参考文献
Gerecs; Windholz
Acta Chimica Academiae Scientiarum Hungaricae, 1958 , vol. 14, p. 417,418
Full Text Show Details
Ashley et al.
Journal of the Chemical Society, 1959 , p. 897,901
