4-(4-硝基苯基)吗啉合成路线 (共 20 条)
反应条件
in acetonitrile 72 h; Heating;
参考文献
Synthesis, , # 12 p. 1145 - 1147
反应条件
1: NEt3 / CH2Cl2 / 0.17 h / -15 °C 2: 100 percent / acetonitrile / 24 h / Heating View Scheme
参考文献
Synthesis, , # 12 p. 1145 - 1147
反应条件
in methanol; water 6.5 h; Ambient temperatureIrradiation;
参考文献
Tetrahedron Letters, , vol. 25, # 37 p. 4147 - 4150
反应条件
in pyridine T=80°C; 5 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 55, # 7 p. 2174 - 2180
反应条件
sulfuric acid; nitric acid T=0°C; 2 h;
参考文献
Heterocycles, , vol. 27, # 2 p. 371 - 376
反应条件
potassium carbonate 8 h; Heating; Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 22, p. 403 - 404
Zhurnal Organicheskoi Khimii, , vol. 22, # 2 p. 455 - 456
反应条件
1: 61 percent / Fe-HCl / H2O / 4 h / Heating View Scheme
参考文献
Kmonicek, Vojtech; Svatek, Emil; Holubek, Jiri; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 4 p. 937 - 947
反应条件
potassium permanganate; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane T=20°C; 11 h; Heating / reflux;
参考文献
MERCK PATENT GMBH
Patent: WO2006/34789 A1, 2006 ;
Location in patent: Page/Page column 41 ;
反应条件
potassium permanganate; sodium sulfate in water; 4-(dicyanomethylene)-2-methyl-6-(4-dimethylaminostyryl)-4H-pyran
参考文献
Aventis Pharma Deutschland GmbH
Patent: EP1571154 A1, 2005 ;
反应条件
palladium on activated charcoal; hydrogen in methanol T=20°C;
参考文献
US2013/45977 A1, ;
Paragraph 0215; 0216; 0217; 0218 ;