3-(2-甲酰基苯基)-2-(E)-丙烯酸叔丁酯合成路线 （共 5 条）
反应条件
potassium chloride; tetra-n-butylammonium acetate; palladium diacetate; potassium carbonate in N,N-dimethyl-formamide T=20 - 90°C; 12.0833 h; Inert atmosphere;
参考文献
Fustero, Santos; Moscardo, Javier; Sanchez-Rosello, Maria; Rodriguez, Elsa; Barrio, Pablo
Organic Letters, 2010 , vol. 12, # 23 p. 5494 - 5497
反应条件
potassium carbonate; [Cl2Pd(COD)]; 1,4-bis(2-hydroxy-3,5-di-tert-butylbenzyl)piperazine in methanol T=60°C; Mizoroki-Heck coupling reaction; 3 h;
参考文献
Mohanty, Sasmita; Suresh; Balakrishna, Maravanji S.; Mague, Joel. T.
Tetrahedron, 2008 , vol. 64, # 1 p. 240 - 247
反应条件
sodium hydroxide in dichloromethane; water T=-5°C; 2.5 h; Large scale reaction; chemoselective reaction;
参考文献
Organic Process Research and Development, , vol. 13, # 4 p. 710 - 715
反应条件
in dichloromethane Wittig reaction;
参考文献
Organic Process Research and Development, , vol. 13, # 4 p. 710 - 715
反应条件
trifluoroacetic acid in ethanol
参考文献
GLAXO S.P.A.
Patent: US4801599 A1, 1989 ;
