1-(氯甲基)-3,5-二[[(叔丁基)二甲基硅烷基]氧基]苯合成路线 （共 3 条）
反应条件
1: 83 percent / xylene / 10 h / Heating 2: 1.) n-BuLi / 1.) benzene, 30 min 2.) benzene, 4 h 3: 40percent aq. HF / acetonitrile / 4 h / Ambient temperature View Scheme
参考文献
Cardona, Luz; Fernandez, Isabel; Garcia, Begona; Pedro, Jose R.
Tetrahedron, 1986 , vol. 42, # 10 p. 2725 - 2730
反应条件
1.1: 86.1 percent / NaI / 6 h / 135 °C 2.1: NaH / tetrahydrofuran / 2 h / -55 - 0 °C 2.2: 50.8 percent / tetrahydrofuran / 24 h / -55 - 0 °C 3.1: 79 percent / hydrochloric acid / ethanol / 26 h / 20 °C View Scheme
参考文献
Takaya, Yoshiaki; Terashima, Kenji; Ito, Junko; He, Yue-Hua; Tateoka, Maki; Yamaguchi, Naho; Niwa, Masatake
Tetrahedron, 2005 , vol. 61, # 43 p. 10285 - 10290
反应条件
1: 83 percent / xylene / 10 h / Heating 2: 1.) n-BuLi / 1.) benzene, 30 min 2.) benzene, 4 h 3: 40percent aq. HF / acetonitrile / 4 h / Ambient temperature View Scheme
参考文献
Cardona, Luz; Fernandez, Isabel; Garcia, Begona; Pedro, Jose R.
Tetrahedron, 1986 , vol. 42, # 10 p. 2725 - 2730
