in ethanol 1 h; Ambient temperature;

in ethyl acetate T=5 - 20°C; 1.41667 h;

trichlorophosphate

in water; acetone T=40°C; other substituting agents, var. solvents, var. time; Rate constant;

T=20°C;

1.1: lithium hydroxide hydrate / water / 20 h / 20 °C 1.2: 24 h / 100 °C 1.3: pH 3 2.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 0.5 h / 0 °C 3.1: tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate / 1,4-dioxane; water / 95 °C 4.1: hydrazine hydrate / ethanol / 80 - 100 °C View Scheme

暂无反应条件数据

ethanol T=170 - 180°C; im Rohr;

T=100°C; im Rohr;