1-十二烷基-4-甲基苯合成路线 （共 10 条）
反应条件
Me4-DACH; magnesium; cobalt(II) chloride in tetrahydrofuran
T=0°C; 3 h;
参考文献
SALTIGO GMBH
Patent: US2009/247764 A1, 2009 ;
Location in patent: Page/Page column 11 ;
反应条件
anhydrous iron chloride; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran
T=0°C; 8 h; Inert atmosphere;
参考文献
Czaplik, Waldemar Maximilian; Mayer, Matthias; Von Wangelin, Axel Jacobi
Angewandte Chemie - International Edition, 2009 , vol. 48, # 3 p. 607 - 610
反应条件
Me4-DACH; magnesium; cobalt(II) chloride in tetrahydrofuran
T=0°C; 3 h; Product distribution / selectivity;
参考文献
SALTIGO GMBH
Patent: US2009/247764 A1, 2009 ;
Location in patent: Page/Page column 11 ;
反应条件
Fe(acac)3; N,N,N',N,-tetramethylethylenediamine; 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane in tetrahydrofuran
T=0°C; 1.33333 h;
参考文献
Cahiez, Gerard; Habiak, Vanessa; Duplais, Christophe; Moyeux, Alban
Angewandte Chemie - International Edition, 2007 , vol. 46, # 23 p. 4364 - 4366
反应条件
butylmethylimidazolium tetrachloroferrate in diethyl ether
T=0 - 20°C;
参考文献
Bica, Katharina; Gaertner, Peter
Organic Letters, 2006 , vol. 8, # 4 p. 733 - 735
反应条件
methanol; kieselguhr; nickel
T=200 - 225°C; P=88260.9 - 114004 Torr; Hydrogenation;
参考文献
Englert et al.
Journal of the American Oil Chemists' Society, 1953 , vol. 30, p. 337
反应条件
Me4-DACH; magnesium; cobalt(II) chloride in tetrahydrofuran
T=0°C; Inert atmosphere;
参考文献
Czaplik, Waldemar Maximilian; Mayer, Matthias; Jacobi Von Wangelin, Axel
Synlett, 2009 , # 18 p. 2931 - 2934
反应条件
1: AlCl3
2: zinc-amalgam; aqueous hydrochloric acid
View Scheme
参考文献
Toda; Kosaka
Kogyo Kagaku Zasshi, 1950 , vol. 53, p. 89,91
Chem.Abstr., 1953 , p. 2717
反应条件
1: AlCl3
2: zinc-amalgam; aqueous hydrochloric acid
View Scheme
参考文献
Toda; Kosaka
Kogyo Kagaku Zasshi, 1950 , vol. 53, p. 89,91
Chem.Abstr., 1953 , p. 2717
反应条件
aluminium trichloride
Erhitzen des gebildeten 1-Methyl-4-lauroyl-benzols mit Hydrazin-hydrat und Natriumaethylat-Loesung;
参考文献
Schmidt; Schoeller
Chemische Berichte, 1941 , vol. 74, p. 258
