1: 87.5 percent / conc. H2SO4 / 0.25 h / Ambient temperature 2: 86.1 percent / 13 percent aq. sodium hypochlorite / acetic acid; acetone / 5 h / 0 °C View Scheme
参考文献
Satoh, Tsuyoshi; Oguro, Kazuko; Shishikura, Jun-ichi; Kanetaka, Naomi; Okada, Reiko; Yamakawa, Koji
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 8 p. 2339 - 2347
pyridine; water; oxygen; triethylamine; pyridine; compound with copper (II)-nitrate in methanol T=25°C; P=1748 Torr; 12 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 55, # 10 p. 3011 - 3018
carbon monoxide; hydrogen; dicobalt octacarbonyl in pyridine T=140°C; P=75005.9 Torr; Yield given. Yields of byproduct given. Title compound not separated from byproducts;