1: CCl3CO2Na 2: 86 percent / CrO3; aq. H5IO6 / acetonitrile / 1.5 h / 20 °C View Scheme
参考文献
Perryman, Michael S.; Harris, Matthew E.; Foster, Jade L.; Joshi, Anushka; Clarkson, Guy J.; Fox, David J.
Chemical Communications, 2013 , vol. 49, # 85 p. 10022 - 10024
triphenylphosphine; diazomethyl-trimethyl-silane; [rhodium(I)chloride(triphenylphosphine)3] in tetrahydrofuran; isopropyl alcohol (Ar); addn. of 2-propanol to soln. of RhCl(PPh3)3 and PPh3 in THF; addn.of hydrocinnamaldehyde and then trimethylsilyldiazomethane, evolution o f gas; stirring at room temp., TLC analysis; slow addn. of pinacolborane; stirring at room temp.; TLC analysis, not isolated;
参考文献
Journal of Organometallic Chemistry, , vol. 690, # 23 p. 5198 - 5205
