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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯丙醛
合成路线
（共 954 条）
104-53-0
苯丙醛
→
反应条件
1588-44-9
6-苯基-1-己烯
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C 2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 2.5 h / 0 - 25 °C / Inert atmosphere 2.2: 760.05 Torr / Inert atmosphere 2.3: 0.75 h View Scheme
参考文献
Graham, Thomas J. A.; Poole, Thomas H.; Reese, Charles N.; Goess, Brian C.
Journal of Organic Chemistry, 2011 , vol. 76, # 10 p. 4132 - 4138
104-53-0
苯丙醛
+
100-63-0
苯肼
→
反应条件
16886-10-5
3-苄基吲哚
反应条件
sulfuric acid in tetrahydrofuran Fischer indolization; 3 h; Heating;
参考文献
Angelovski, Goran; Keraenen, Mark D.; Linnepe, Petra; Grudzielanek, Stefan; Eilbracht, Peter
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 10-11 p. 1193 - 1199
104-53-0
苯丙醛
+
59-88-1
盐酸苯肼
→
反应条件
16886-10-5
3-苄基吲哚
反应条件
1,3-bis(3-sulfopropyl)-1H-imidazol-3-ium trifluoromethanesulfonate in water T=100°C; Fischer Indole Synthesis; 0.333333 h; Microwave irradiationGreen chemistry;
参考文献
Li, Bai Lin; Zhong, Ai Guo; Xu, Dan-Qian
Journal of Fluorine Chemistry, 2012 , vol. 144, p. 45 - 50,6
104-53-0
苯丙醛
+
615-43-0
2-碘苯胺
→
反应条件
16886-10-5
3-苄基吲哚
反应条件
1: 2-iodo aniline With AmPhos; palladium dichloride in 1,4-dioxane T=20°C; 0.166667 h; Inert atmosphere; 2: 3-phenyl-propionaldehyde With caesium acetate in 1,4-dioxane T=120°C; 0.666667 h; Inert atmosphereMicrowave irradiation;
参考文献
Karuvalam, Ranjith P.; Haridas, Karickal R.; Sajith, Ayyiliath M.; Muralidharan, Arayambath
Tetrahedron Letters, 2013 , vol. 54, # 37 p. 5126 - 5129
104-53-0
苯丙醛
+
88-67-5
邻碘苯甲酸
→
反应条件
16886-10-5
3-苄基吲哚
反应条件
1: 2-iodo benzoic acid With sodium azide; benzyl chloroformate; sodium t-butanolate in N,N-dimethyl-formamide T=75°C; 5 h; 2: 3-phenyl-propionaldehyde With 1,4-diaza-bicyclo[2.2.2]octane; palladium diacetate in N,N-dimethyl-formamide T=120°C; 16 h; Further stages.;
参考文献
Leogane, Olivier; Lebel, Helene
Angewandte Chemie - International Edition, 2008 , vol. 47, # 2 p. 350 - 352
104-53-0
苯丙醛
+
6091-44-7
哌啶盐酸盐
→
反应条件
21924-11-8
反应条件
1: 3-phenyl-propionaldehyde With 1-hydroxy-pyrrolidine-2,5-dione; oxygen; [Co(O2CCH3)2]*4H2O; sodium hydrogencarbonate in acetonitrile T=20°C; P=760.051 Torr; 1 h; Molecular sieve; 2: tetrahydropyridine hydrochloride in acetonitrile T=20°C; Molecular sieve;
参考文献
Yao, Haoyi; Yamamoto, Kana
Chemistry - An Asian Journal, 2012 , vol. 7, # 7 p. 1542 - 1545
104-53-0
苯丙醛
→
反应条件
21924-11-8
反应条件
1: 73 percent / 2,2'-azobis[2-(2-imidazolin-2-yl)propane] dihydrochloride; cetyltrimethylammonium bromide / H2O / 18 h / 50 °C 2: H2O / 0.5 h / 50 °C View Scheme
参考文献
Toledo, Hila; Pisarevsky, Evgeni; Abramovich, Adi; Szpilman, Alex M.
Chemical Communications, 2013 , vol. 49, # 39 p. 4367 - 4369
104-53-0
苯丙醛
→
反应条件
20845-80-1
反应条件
1: 80 percent / 1.) LDA / tetrahydrofuran / -65 °C 2: 55 percent / EtMgBr / tetrahydrofuran / 1.5 h / -78 - -45 °C / other reagent (LDA) View Scheme
参考文献
Shono, Tatsuya; Kise, Naoki; Yamazaki, Akira; Ohmizu, Hiroshi
Tetrahedron Letters, 1982 , vol. 23, # 15 p. 1609 - 1612
104-53-0
苯丙醛
→
反应条件
2235-83-8
5-苯基戊烷-2-酮
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C 1.2: 90 percent / tetrahydrofuran; hexane / 1 h / -78 °C 2.1: 91 percent / TBAF / tetrahydrofuran / 0.17 h / 20 °C 3.1: 85 percent / DMAP; pyridine / 0.5 h / 20 °C 4.1: H2O / NaAuCl4*2H2O / methanol / 2 h / Heating 5.1: SmI2; ethyl acrylate; MeOH View Scheme
参考文献
Meyers, A. I.; Edwards, Philip D.; Bailey, Thomas R.; Jagdmann, G. Erik
Journal of Organic Chemistry, 1985 , vol. 50, # 7 p. 1019 - 1026
104-53-0
苯丙醛
+
78-94-4
→
反应条件
22289-05-0
反应条件
1,4-diaza-bicyclo[2.2.2]octane in tetrahydrofuran 85 h; Ambient temperature;
参考文献
Basavaiah, Deevi; Gowriswari, Vellanki V. L.; Dharma Rao, Polisetti; Bharathi, Tirumala K.
Journal of Chemical Research, Miniprint, 1995 , # 7 p. 1656 - 1673
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