Pinhey, John T.; Stoermer, Martin J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 10 p. 2455 - 2460
1: 10-P-5 With sodium hydride in tetrahydrofuran; mineral oil
T=0°C; 1 h; Inert atmosphere;
2: 3-phenyl-propionaldehyde in tetrahydrofuran; mineral oil
T=-78°C; Horner-Wadsworth-Emmons olefination; 12 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
1: With potassium carbonate
Horner-Wadsworth-Emmons olefination; 6 h; Neat (no solvent)high-speed ball milling;
2: With Oxonereg;
12 h; Neat (no solvent)high-speed ball milling; optical yield given as percent dediastereoselective reaction;
参考文献
Shearouse, William C.; Korte, Chelsea M.; Mack, James
Green Chemistry, 2011 , vol. 13, # 3 p. 598 - 601
