1: dimethyl hydrogen phosphite; 3-phenyl-propenal With titanium(IV) isopropylate; 4(1S,2S)-trans-1,2-cyclohexanediol in diethyl ether T=-15°C; 2: acetyl chloride With poly(4-vinyl)pyridine in acetonitrile T=20°C; 3: With Rhizopus arrizhus lipase in phosphate buffer pH=7.0; Title compound not separated from byproducts;
参考文献
Rowe, Bradley J.; Spilling, Christopher D.
Tetrahedron Asymmetry, 2001 , vol. 12, # 12 p. 1701 - 1708
