alphs-戊基-gama-丁内酯合成路线 （共 55 条）
参考文献
OTSUKA KAGAKU KABUSHIKI KAISHA
Patent: EP1178026 A1, 2002 ;
Location in patent: Page 11 ;
反应条件
Na2B4O7; ethylenediaminetetraacetic acid; bis(dibutylethyl)hexamethylenediammonium hydroxide; triethylamine in water T=20°C; pH=10; Electrochemical reaction; Reagent/catalystSolventTemperatureConcentration;
参考文献
US2014/100376 A1, ;
Paragraph 0054-0057 ;
反应条件
hydrogen; nickel in ethanol 24 h;
参考文献
Gurjar, M. K.; Purandare, A. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, p. 554 - 555
反应条件
samarium diiodide in tetrahydrofuran T=0°C; 10 h;
参考文献
Fukuzawa, Shin-ichi; Nakanishi, Akira; Fujinami, Tatsuo; Sakai, Shizuyoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1669 - 1676
反应条件
hydrogen; palladium on activated charcoal in methanol Hydrogenation; lactonization; P=2068.59 Torr; 15 h;
参考文献
Chemical Research in Toxicology, , vol. 8, # 1 p. 34 - 39
反应条件
sodium tetrahydroborate; disodium hydrogenphosphate in methanol 5 h; Ambient temperature;
参考文献
Ballini, Roberto; Petrini, Marino; Rosini, Goffredo
Synthesis, 1987 , # 8 p. 711 - 713
反应条件
1: n-butyl-magnesium chloride With copper (I) cyanide in tetrahydrofuran T=0°C; 0.416667 h; Inert atmosphere; 2: epoxy-4,5 pentanoate de methyle in tetrahydrofuran T=0°C; 1 h; Inert atmosphere; 3: With ammonium chloride in tetrahydrofuran; diethyl ether; water
参考文献
Ugurchieva; Lozanova; Zlokazov; Veselovsky
Russian Chemical Bulletin, 2008 , vol. 57, # 3 p. 657 - 659
反应条件
chloro-trimethyl-silane; tetraethylammonium p-toluenesulfonate in N,N-dimethyl-formamide Ambient temperatureelectroreductive crossed hydrocoupling;
参考文献
Shono, Tatsuya; Ohmizu, Hiroshi; Kawakami, Souta; Sugiyama, Hiroshi
Tetrahedron Letters, 1980 , vol. 21, p. 5029 - 5032
反应条件
2,2'-azo-bisisobutyronitrile in benzene 8 h; Heating;
参考文献
Kraus, George A.; Landgrebe, Kevin
Tetrahedron, 1985 , vol. 41, # 19 p. 4039 - 4046
反应条件
NiI2; samarium diiodide in tetrahydrofuran Addition; 1 h;
参考文献
Machrouhi, Fouzia; Namy, Jean-Louis
Tetrahedron, 1998 , vol. 54, # 37 p. 11111 - 11122
