alphs-戊基-gama-丁内酯合成路线 (共 55 条)
反应条件
dibenzoyl peroxide in benzene Heating;
参考文献
Nakano, Taichi; Kayama, Mikio; Nagai, Yoichiro
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 3 p. 1049 - 1052
反应条件
1: 25 percent / sodium chlorite; 1 mM HCl; sulfamic acid / H2O / 3 h / 20 °C 2: hydrogen / Pd/C / methanol / 15 h / 2068.59 Torr View Scheme
参考文献
Chemical Research in Toxicology, , vol. 8, # 1 p. 34 - 39
反应条件
di-tert-butyl peroxide; zinc dibromide T=180°C; 12 h; Dean-Stark;
参考文献
Tu, Song; Dong, Wan; Yang, Jing; Zhang, Chen; Shen, Youyu
Organic Preparations and Procedures International, 2013 , vol. 45, # 1 p. 72 - 74
反应条件
D-glucose; C. boidinii in phosphate buffer T=20°C; pH=6.0;
参考文献
Tetrahedron Asymmetry, , vol. 12, # 7 p. 1039 - 1046
反应条件
tetraethylammonium p-toluenesulfonate in N,N-dimethyl-formamide cathodic reduction;
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Kashimura, Shigenori
Journal of Chemical Research, Miniprint, 1984 , # 7 p. 1922 - 1935
反应条件
1: 80 percent / propionic acid / 100 - 105 °C 2: 90 percent / aq. KOH / methanol / 4 h / Heating 3: 70 percent / I2, KI / acetonitrile / 24 h / Ambient temperature 4: 85 percent / H2 / Raney nickel / ethanol / 24 h View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 27, p. 554 - 555
反应条件
1: 70 percent / I2, KI / acetonitrile / 24 h / Ambient temperature 2: 85 percent / H2 / Raney nickel / ethanol / 24 h View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 27, p. 554 - 555
反应条件
1: 90 percent / aq. KOH / methanol / 4 h / Heating 2: 70 percent / I2, KI / acetonitrile / 24 h / Ambient temperature 3: 85 percent / H2 / Raney nickel / ethanol / 24 h View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 27, p. 554 - 555
反应条件
in tetrahydrofuran 2 h; Ambient temperature;
参考文献
Kobayashi, Kazuhiro; Sasaki, Akiyoshi; Kanno, Yoshikazu; Suginome, Hiroshi
Tetrahedron, 1991 , vol. 47, # 35 p. 7245 - 7258
反应条件
1: dimethyl malonate, Na, methanol / 3 h / Heating 2: KOH / methanol; H2O / Heating 3: H2SO4 / H2O / 10 h / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 53, # 3 p. 770 - 774