1.1: hydroxylamine hydrochloride / ethanol / 0.67 h / 20 °C 2.1: hydrogenchloride; zinc / ethanol; water / 0.25 h / 20 °C 2.2: 0.25 h / 20 °C View Scheme
1: With potassium carbonate in water T=20°C; 1 h; Inert atmosphere; 2: With 2,4,6-trichloro-1,3,5-triazine in dichloromethane; water T=0°C; 0.5 h; Inert atmosphere; 3: With sodium hydroxide in dichloromethane; water pH=11; Inert atmosphere;
triethylamine in dichloromethane 4 h; Inert atmosphere;
参考文献
Amenta, Valeria; Cook, Joanne L.; Hunter, Christopher A.; Low, Caroline M. R.; Sun, Hongmei; Vinter, Jeremy G.
Journal of the American Chemical Society, 2013 , vol. 135, # 32 p. 12091 - 12100
