反应条件
1: 1.) PMHS, Ti(i-PrO)4 / 1.) THF, reflux, 6 h, 2.) THF, reflux, 1 h 2: TMP, NBS / CHCl3 / 2.5 h / Ambient temperature View Scheme
参考文献
Al-Riyami, Lamyaa; Pineda, Miguel A.; Rzepecka, Justyna; Huggan, Judith K.; Khalaf, Abedawn I.; Suckling, Colin J.; Scott, Fraser J.; Rodgers, David T.; Harnett, Margaret M.; Harnett, William
Journal of Medicinal Chemistry, 2013 , vol. 56, # 24 p. 9982 - 10002