反应条件
1.1: dibenzoyl peroxide; N-bromosuccinmide / chloroform / 3.5 h / 60 - 65 °C / |Large scale 2.1: chloroform / 3 h / 20 - 25 °C / |Large scale 3.1: hydrogenchloride; water / water / 5 h / 90 - 95 °C / |Large scale 4.1: thionyl chloride / 24 h / 80 °C / |Large scale 5.1: potassium carbonate / isopropyl alcohol / 0.25 h / 20 °C / |Large scale 5.2: 1.5 h / 20 °C / |Large scale 5.3: 0.5 h / 20 °C / |Large scale View Scheme
参考文献
Kompella, Amala; Adibhatla, Bhujanga Rao Kalisatya; Muddasani, Pulla Reddy; Rachakonda, Sreenivas; Gampa, Venugopala Krishna; Dubey, Pramod Kumar
Organic Process Research and Development, 2012 , vol. 16, # 11 p. 1794 - 1804
