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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-溴苯甲醚
合成路线
（共 1936 条）
104-92-7
4-溴苯甲醚
+
628-08-0
反-2-丁烯醋酸酯
→
反应条件
39831-53-3
+
18272-83-8
反应条件
NiBr2bipy; tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide T=70°C; i = 250 mA, nickel-sponge cathode; Yield given. Yields of byproduct given;
参考文献
Mayer, Matthias; Czaplik, Waldemar M.; Von Wangelin, Axel Jacobi
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 13 p. 2147 - 2152
104-92-7
4-溴苯甲醚
+
6737-11-7
3-丁烯-2-醋酸
→
反应条件
39831-53-3
+
18272-83-8
反应条件
1: 1-bromo-4-methoxy-benzene With magnesium; lithium chloride in tetrahydrofuran T=20°C; 2 h; Inert atmosphere; 2: With iron (III) acetylacetonate in tetrahydrofuran T=0°C; 0.0833333 h; Inert atmosphere; 3: 3-buten-2-yl acetate in tetrahydrofuran T=0 - 20°C; 2 h; Inert atmosphere; regioselective reaction;
参考文献
Mayer, Matthias; Czaplik, Waldemar M.; Von Wangelin, Axel Jacobi
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 13 p. 2147 - 2152
104-92-7
4-溴苯甲醚
→
反应条件
18272-83-8
+
18322-84-4
反应条件
potassium carbonate; bis(1,1-diphenylphosphino)methane; palladium diacetate in tetrahydrofuran; water 20 h; Heating; Product distribution; Further Variations:Reagents;
参考文献
Yamamoto, Yasunori; Takada, Shingo; Miyaura, Norio
Chemistry Letters, 2006 , vol. 35, # 12 p. 1368 - 1369
530-48-3
1,1-二苯乙烯
+
104-92-7
4-溴苯甲醚
→
反应条件
18648-74-3
反应条件
bis(η3-allyl-μ-chloropalladium(II)); Tedicyp; potassium carbonate in N,N-dimethyl-formamide T=130°C; Heck vinylation; 20 h;
参考文献
Berthiol, Florian; Doucet, Henri; Santelli, Maurice
European Journal of Organic Chemistry, 2003 , # 6 p. 1091 - 1096
530-48-3
1,1-二苯乙烯
+
104-92-7
4-溴苯甲醚
+
103-30-0
反式-1,2-二苯乙烯
→
反应条件
18648-74-3
反应条件
palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine in N,N-dimethyl-formamide T=130°C; Heck reaction; 5 h; Inert atmosphere; optical yield given as percent deregioselective reaction;
参考文献
Limberger, Jones; Poersch, Silvia; Monteiro, Adriano L.
Journal of the Brazilian Chemical Society, 2011 , vol. 22, # 7 p. 1389 - 1394
104-92-7
4-溴苯甲醚
+
5323-87-5
3-乙氧基-2-环己烯-1-酮
→
反应条件
17159-98-7
反应条件
1: 1-bromo-4-methoxy-benzene With n-butyllithium in diethyl ether; hexane T=0°C; 2 h; 2: 3-ethoxy-2-cyclohexen-1-one in diethyl ether; hexane T=-70°C; 2 h; 3: With hydrogenchloride in diethyl ether; hexane T=20°C; 1.5 h;
参考文献
Zimmerman, Howard E.; Nesterov, Evgueni E.
Journal of the American Chemical Society, 2003 , vol. 125, # 18 p. 5422 - 5430
104-92-7
4-溴苯甲醚
+
930-68-7
2-环己烯-1-酮
→
反应条件
17159-98-7
反应条件
N,N'-dimethyl-N,N'-propyleneurea; C13H11F9O4Pd; lithium carbonate; [(t-Bu)3PH]BF4 T=120°C; Heck Reaction; 36 h; Inert atmosphereGloveboxSchlenk technique;
参考文献
Wu, Xiaojin; Zhou, Jianrong
Chemical Communications, 2013 , vol. 49, # 42 p. 4794 - 4796
104-92-7
4-溴苯甲醚
→
反应条件
18855-13-5
反应条件
1: 91 percent / aq. Na2CO3 / Pd(PPh3)4 / toluene / 90 - 100 °C 2: 96 percent / BBr3 / CH2Cl2 / 20 °C View Scheme
参考文献
Moorthy, Jarugu Narasimha; Venkatakrishnan, Parthasarathy; Samanta, Subhas
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 9 p. 1354 - 1357
→
反应条件
2362-68-7
反应条件
cesium fluoride in toluene Stille cross-coupling reaction; Heating;
参考文献
Haemmerle, Johanna; Schnuerch, Michael; Stanetty, Peter
Synlett, 2007 , # 19 p. 2975 - 2978
→
反应条件
17064-22-1
反应条件
copper(l) iodide; potassium carbonate; palladium diacetate in N,N-dimethyl-formamide T=150°C; 0.25 h; microwave irradiation;
参考文献
Besselievre, Francois; Mahuteau-Betzer, Florence; Grierson, David S.; Piguel, Sandrine
Journal of Organic Chemistry, 2008 , vol. 73, # 8 p. 3278 - 3280
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