1: With [resin-CH2N(CH3)3]2CO3 in water; N,N-dimethyl-formamide T=80°C; Suzuki coupling; 16 h; 2: With [resin-CH2N(CH3)3]2CO3; 4-{[(9-anthrylmethyl)amino]carbonyl}phenylboronic acid in water; N,N-dimethyl-formamide T=80°C; 3: With maleimido-CH2-PS resin in water; N,N-dimethyl-formamide T=90°C; 10 h;
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1: 1-bromo-4-methoxy-benzene With magnesium in tetrahydrofuran 1 h; Inert atmosphereReflux; 2: carbonic acid dimethyl ester in tetrahydrofuran 4 h; Inert atmosphereReflux; 3: With water in tetrahydrofuran T=20°C; Inert atmosphere;
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Guieu, Samuel; Rocha, Joao; Silva, Artur M.S.
Tetrahedron Letters, 2013 , vol. 54, # 22 p. 2870 - 2873
1: 1-bromo-4-methoxy-benzene With magnesium in tetrahydrofuran Reflux; 2: methyl 4-(N-tert-butoxycarbonyl-(5S)-methyl-(2S)-pyrrolidinylmethoxy)benzoate in tetrahydrofuran T=20°C; Reflux;
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Horn, Markus; Mayr, Herbert
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tetrabutylammomium bromide; potassium carbonate; palladium dichloride in water T=175°C; Heck reaction; P=14480.5 Torr; 0.25 h; Microwave irradiationInert atmosphere;
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