(+)-(3As,6as)-3a,6a-二氢-2,2-二甲基-4H-环戊并-1,3-二氧代-4-酮合成路线 （共 95 条）
参考文献
Ali, Syed Mashhood; Ramesh, Kakarla; Borchardt, Ronald T.
Tetrahedron Letters, 1990 , vol. 31, # 11 p. 1509 - 1512
反应条件
1: 90 percent / 1,5-diazabicyclo<5.4.0>undecene-5 / benzene / 3 h / Heating
2: 60 percent / sodium methoxide / methanol / 3 h / Heating
View Scheme
参考文献
Ohrui, Hiroshi; Konno, Masao; Meguro, Hiroshi
Agricultural and Biological Chemistry, 1987 , vol. 51, # 2 p. 625 - 626
反应条件
1: 1.) NaH
2: 56 percent
3: toluene / 192 h / Heating
5: 90 percent / Al(iBu)2H
6: H(+)
View Scheme
参考文献
Bestmann, Hans Juergen; Moenius, Thomas
Angewandte Chemie, 1986 , vol. 98, # 11 p. 1007 - 1008
反应条件
1: 56 percent
2: toluene / 192 h / Heating
4: 90 percent / Al(iBu)2H
5: H(+)
View Scheme
参考文献
Bestmann, Hans Juergen; Moenius, Thomas
Angewandte Chemie, 1986 , vol. 98, # 11 p. 1007 - 1008
反应条件
1: toluene / 192 h / Heating
3: 90 percent / Al(iBu)2H
4: H(+)
View Scheme
参考文献
Bestmann, Hans Juergen; Moenius, Thomas
Angewandte Chemie, 1986 , vol. 98, # 11 p. 1007 - 1008
反应条件
T=-78°C; Horner-Wadsworth reaction; 2.5 h;
参考文献
Brooks, Allen F.; Garcia, George A.; Showalter, H.D. Hollis
Tetrahedron Letters, 2010 , vol. 51, # 32 p. 4163 - 4165
反应条件
1-aza-bicyclo[2.2.2]octane; sodium periodate; methanesulfonamide; K2Os(OH)4; potassium carbonate; sodium sulfite; potassium hexacyanoferrate(III)
Yield given. Multistep reaction;
参考文献
Armstrong, Alan; Hayter, Barry R.
Tetrahedron Asymmetry, 1997 , vol. 8, # 10 p. 1677 - 1684
反应条件
n-butyllithium
1.) THF, hexane, -78 deg C, 15 min, 2.) THF, hexane, from -78 deg C to RT, 1 h 20 min; Yield given. Multistep reaction;
参考文献
Hudlicky; Natchus; Nugent
Synthetic Communications, 1992 , vol. 22, # 1 p. 151 - 157
参考文献
Bestmann, Hans Juergen; Moenius, Thomas
Angewandte Chemie, 1986 , vol. 98, # 11 p. 1007 - 1008
反应条件
1: 90 percent / Al(iBu)2H
2: H(+)
View Scheme
参考文献
Bestmann, Hans Juergen; Moenius, Thomas
Angewandte Chemie, 1986 , vol. 98, # 11 p. 1007 - 1008
