3-(三氟甲基)吡啶-2-硫醇合成路线 (共 4 条)
反应条件
Lawesson's reagent in toluene
参考文献
Dunn
Journal of Fluorine Chemistry, 1999 , vol. 93, # 2 p. 153 - 157
反应条件
1: 69 percent / H2SO4, NaNO2 / H2O / 1 h / 70 °C 2: 71 percent / Lawesson's reagent / toluene View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 93, # 2 p. 153 - 157
反应条件
β-mercaptopropionic acid methyl ester; sodium methylate multistep reaction; conversion of halopyridines into thiones; other halopyridines;
参考文献
Journal fuer Praktische Chemie/Chemiker-Zeitung, , vol. 334, # 2 p. 119 - 125
反应条件
ammonium hydroxide; acetic acid in water
参考文献
Ishihara Sangyo Kaisha
Patent: US4744814 A1, 1988 ;