mercury(II) oxide
byproducts: CO2; NF2COCl condensed to freshly made yellow HgO, -78°C, 2.5h, in pyrex vessel; fractionated condensation at -138°C (sepn. from NF2COCl), addn. of 5A molecular sieve (removing HNF2);
Gmelin Handbook: C: MVol.D3, 3.2.4, page 124 - 125
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North American Aviation Inc.,
Patent: FR1319900 , 1963 ;
C.A., 1963 , vol. 59, p. 8602
Fehling soln. in water
detected in gaseous mixt.;;
参考文献
Ruff, O.; Staub, L.
Z. Anorg. Chem., 1931 , vol. 198, p. 32 - 38
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Gmelin Handbook: F: SVol.1, 73, page 249 - 251
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Staub, L.
Diss. Breslau T. H. 1932
in dichloromethane
all manipulations under N2; condensing FSO2NF2 into CH2Cl2 (-55°C), adding dropwise freshly distd. NHEt2 (-55°C, stirring, 2 h), color changing to yellowish; allowing to warm to room temp. (overnight), removing the solvent, distg. (water bath);
参考文献
Roesky, H. W.; Otten, U.; Oberhammer, H.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1986 , vol. 539, p. 191 - 194
Sawton, E. A.; Weber, J. Q.
Journal of the American Chemical Society, 1959 , vol. 81, p. 4755
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Gmelin Handbook: C: MVol.D1, 45.8.3.2, page 416 - 416
