二-(4-甲苯基)-二砜合成路线 （共 61 条）
反应条件
chlorosulphuric acid; chloroform
参考文献
Huntress; Autenrieth
Journal of the American Chemical Society, 1941 , vol. 63, p. 3446
反应条件
monobromonitromethane in water
T=24°C; 2 h;
参考文献
Fishwick, Brian R.; Rowles, David K.; Stirling, Charles J. M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1171 - 1180
反应条件
aci-anion nitromethane sodium salt in ethanol; water
T=23°C; 24 h; Further byproducts given;
参考文献
Fishwick, Brian R.; Rowles, David K.; Stirling, Charles J. M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1171 - 1180
参考文献
Barr; Ziegler; Connor
Journal of the American Chemical Society, 1941 , vol. 63, p. 106
反应条件
2,6-dimethylpyridine in methanol
T=20°C; 48 h;
参考文献
Pigou, Paul E.; Stirling, Charles J. M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 725 - 730
反应条件
tert-butyl phenylperoxyacetate in benzene
T=70°C; 40 h; Further byproducts given;
参考文献
da Silva Correa, Carlos M.M.; Oliveira, Maria Augusta B.C.S.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 811 - 814
反应条件
N-chlorosuccinimide-dimethylsulfide complex; triethylamine in methanol; dichloromethane
-5 deg C, then RT, 2 h;
参考文献
Furukawa; Nishikawa; Inaba; et al.
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 3 p. 623 - 628
反应条件
1: 0.62 g / azoisobutyronitrile / CCl4 / 9 h / Heating
2: 25 mg / t-butyl phenylperacetate / benzene / 40 h / 70 °C
View Scheme
参考文献
da Silva Correa, Carlos M.M.; Oliveira, Maria Augusta B.C.S.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 811 - 814
反应条件
copper acetylacetonate in tert-butyl alcohol
5 h; Heating;
参考文献
Hatjiarapoglou, Lazaros; Varvoglis, Anastassios; Alcock, Nathaniel W.; Pike, Graham A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2839 - 2846
反应条件
1: 81 percent / t-BuOCl / CH2Cl2 / 2 h / Ambient temperature; chloramine-T, CH2Cl2, RT
2: 12 percent / Et3N / CH2Cl2 / 2 h / Ambient temperature
View Scheme
参考文献
Furukawa; Nishikawa; Inaba; et al.
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 3 p. 623 - 628
