二-(4-甲苯基)-二砜合成路线 (共 61 条)
反应条件
calcium carbonate
T=20°C; 16 h;
参考文献
Pigou, Paul E.; Stirling, Charles J. M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 725 - 730
反应条件
in N,N-dimethyl-formamide
T=20°C; 48 h;
参考文献
Pigou, Paul E.; Stirling, Charles J. M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 725 - 730
反应条件
1: BrCH2NO2 / aq. ethanol
2: aq. ethanol
View Scheme
参考文献
Fishwick, Brian R.; Rowles, David K.; Stirling, Charles J. M.
Journal of the Chemical Society, Chemical Communications, 1983 , # 15 p. 835 - 836
反应条件
(i) Na, toluene, (ii)/BRN= 1719345/; Multistep reaction;
参考文献
Ziegler,G.R. et al.
Journal of the American Chemical Society, 1963 , vol. 85, p. 1648 - 1651
反应条件
in ethanol; water
T=24°C; 2 h;
参考文献
Fishwick, Brian R.; Rowles, David K.; Stirling, Charles J. M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1171 - 1180
反应条件
2,2'-azo-bisisobutyronitrile in tetrachloromethane
9 h; Heating; Further byproducts given;
参考文献
da Silva Correa, Carlos M.M.; Oliveira, Maria Augusta B.C.S.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 811 - 814
反应条件
in ethanol; water
T=23°C; 24 h; Further byproducts given;
参考文献
Fishwick, Brian R.; Rowles, David K.; Stirling, Charles J. M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1171 - 1180
反应条件
calcium carbonate
T=20°C; 16 h;
参考文献
Pigou, Paul E.; Stirling, Charles J. M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 725 - 730
反应条件
copper in tetrachloromethane
6 h; Heating;
参考文献
da Silva Correa, Carlos M.M.; Oliveira, Maria Augusta B.C.S.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 811 - 814
反应条件
2,2'-azo-bisisobutyronitrile in tetrachloromethane
9 h; Heating; Further byproducts given;
参考文献
da Silva Correa, Carlos M.M.; Oliveira, Maria Augusta B.C.S.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 811 - 814