N-(9-芴甲氧羰基)-D-谷氨酸合成路线 （共 8 条）
反应条件
triethylsilane; trifluoroacetic acid in dichloromethane 0.333333 h; Ambient temperature;
参考文献
Mehta, Anita; Jaouhari, Rabih; Benson, Timothy J.; Douglas, Kenneth T.
Tetrahedron Letters, 1992 , vol. 33, # 37 p. 5441 - 5444
反应条件
triethylamine in water; acetonitrile T=20°C; 2 h;
参考文献
Ibrahim, Tarek S.; Tala, Srinivasa R.; El-Feky, Said A.; Abdel-Samii, Zakaria K.; Katritzky, Alan R.
Synlett, 2011 , # 14 art. no. S03511ST, p. 2013 - 2016
反应条件
in acetonitrile T=20°C; pH=9.2; 0.25 h; aq. borate buffer;
参考文献
Journal of the Chinese Chemical Society, , vol. 58, # 4 p. 509 - 515
反应条件
1: triethylamine / dichloromethane / 2 h / 10 °C 2: triethylamine / water; acetonitrile / 2 h / 20 °C View Scheme
参考文献
Synlett, , # 14 art. no. S03511ST, p. 2013 - 2016
反应条件
dicyclohexyl-carbodiimide in tetrahydrofuran
参考文献
Liu, Gang; Zhao, Nan; Ma, Yao
Patent: US2013/143826 A1, 2013 ;
Location in patent: Page/Page column ;
反应条件
potassium carbonate; dicyclohexyl-carbodiimide 1.) THF, 23 h, 2.) THF, 3.5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kelly, Robert C.; Gebhard, I.; Wicnienski, N.
Journal of Organic Chemistry, 1986 , vol. 51, # 24 p. 4590 - 4594
反应条件
1: 1.) N,N'dicyclohexylcarbodiimide, 2.) potassium carbonate / 1.) THF, 23 h, 2.) THF, 3.5 h 2: 85 percent / sulfur acid / CH2Cl2 / 6 h / 25 °C / 1499.7 Torr 3: 100 percent / ammonium formate / 10percent Pd/C / methanol; tetrahydrofuran / 0.33 h / 0 - 5 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 24 p. 4590 - 4594
反应条件
CLEA-Alcalase in tert-butyl methyl ether T=50°C; 16 h; Molecular sieve;
参考文献
Nuijens, Timo; Cusan, Claudia; Kruijtzer, John A. W.; Rijkers, Dirk T. S.; Liskamp, Rob M. J.; Quaedflieg, Peter J. L. M.
Synthesis, 2009 , # 5 p. 809 - 814
