1: bislt;(tert-butylphenyl)phosphinogt;phosphinic anhydride With potassium naphthalenide in tetrahydrofuran
T=-78°C; 2 h;
2: With sulfur in tetrahydrofuran
14 h;
3: methyl iodide in tetrahydrofuran
2 h;
参考文献
Nycz, Jacek; Rachon, Janusz
Phosphorus, Sulfur and Silicon and Related Elements, 2000 , vol. 161, p. 39 - 59
→
反应条件
1: in tetrahydrofuran
T=-78°C; 3 h;
2: With air in tetrahydrofuran
参考文献
Nycz, Jacek E.; Musiol, Robert
Heteroatom Chemistry, 2006 , vol. 17, # 4 p. 310 - 316
