2,2,6,6-tetramethyl-piperidine-N-oxyl in benzene Irradiation (UV/VIS); N2; Sn-compd. soln. irradiation with 300 W high-pressure Hg lamp throughsatd. aq. CuSO4 soln. (280 nm) for 3 h, solvent evapn. (reduced pressur e);
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Takuwa, Akio; Kanaue, Takashi; Yamashita, Koichi; Nishigaichi, Yutaka
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 7 p. 1309 - 1314
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in further solvent(s) byproducts: 3-methyl-1-butene (20percent); addn. of stannane to soln. of BCl3 (1.3 equiv. in 1,1,2,2-tetrachloroethane) at -40°C, stirring for 10 min at -40°C; trap-to-trap distn. (removing solvent at -50°C, distn. of productat -80°C); NMR spectroscopy;
参考文献
Le Serre, Stephanie; Guillemin, Jean-Claude
Organometallics, 1997 , vol. 16, # 26 p. 5844 - 5848
Lipshutz, Bruce H.; Crow, Robert; Dimock, Stuart H.; Ellsworth, Edmund L.; Smith, Robin A. J.; Behling, James R.
Journal of the American Chemical Society, 1990 , vol. 112, # 10 p. 4063 - 4064
