3,6-二氯-2-甲氧基苯甲酸氯合成路线 （共 10 条）
反应条件
1: triethylamine / dichloromethane / 16 h 2: water / acetonitrile / 392 h / 35 °C / |Darkness View Scheme
参考文献
MONSANTO TECHNOLOGY LLC; MORGENSTERN, David, A.
Patent: WO2013/55944 A2, 2013 ;
反应条件
thionyl chloride; N,N-dimethyl-formamide in chloroform
Heating;
参考文献
Pilyugin; Sapozhnikov; Sapozhnikova
Russian Journal of General Chemistry, 2004 , vol. 74, # 5 p. 738 - 743
反应条件
1: tetrahydrofuran / 28 h / 35 °C / |Sealed tube; |UV-irradiation
2: thionyl chloride / 2.5 h / 80 °C
View Scheme
参考文献
MONSANTO TECHNOLOGY LLC; MORGENSTERN, David, A.
Patent: WO2013/55944 A2, 2013 ;
反应条件
1: tetrahydrofuran / 168 h / 35 °C / |Sealed tube; |UV-irradiation
2: thionyl chloride / 2.5 h / 80 °C
View Scheme
参考文献
MONSANTO TECHNOLOGY LLC; MORGENSTERN, David, A.
Patent: WO2013/55944 A2, 2013 ;
反应条件
1: water / acetonitrile / 392 h / 35 °C / |Darkness
2: thionyl chloride / 2.5 h / 80 °C
View Scheme
参考文献
MONSANTO TECHNOLOGY LLC; MORGENSTERN, David, A.
Patent: WO2013/55944 A2, 2013 ;
反应条件
1: water / acetonitrile / 392 h / 35 °C / |Sealed tube; |UV-irradiation
2: thionyl chloride / 2.5 h / 80 °C
View Scheme
参考文献
MONSANTO TECHNOLOGY LLC; MORGENSTERN, David, A.
Patent: WO2013/55944 A2, 2013 ;
反应条件
1: water / acetonitrile / 392 h / 35 °C / |Sealed tube; |Darkness
2: thionyl chloride / 2.5 h / 80 °C
View Scheme
参考文献
MONSANTO TECHNOLOGY LLC; MORGENSTERN, David, A.
Patent: WO2013/55944 A2, 2013 ;
反应条件
1: water / acetonitrile / 294 h / 35 °C / |Sealed tube; |Darkness
2: thionyl chloride / 2.5 h / 80 °C
View Scheme
参考文献
MONSANTO TECHNOLOGY LLC; MORGENSTERN, David, A.
Patent: WO2013/55944 A2, 2013 ;
反应条件
1: water; acetonitrile / 392 h / 35 °C / |UV-irradiation
2: thionyl chloride / 2.5 h / 80 °C
View Scheme
参考文献
MONSANTO TECHNOLOGY LLC; MORGENSTERN, David, A.
Patent: WO2013/55944 A2, 2013 ;
反应条件
1: water / acetonitrile / 98 h / 35 °C / |Sealed tube; |Darkness
2: thionyl chloride / 2.5 h / 80 °C
View Scheme
参考文献
MONSANTO TECHNOLOGY LLC; MORGENSTERN, David, A.
Patent: WO2013/55944 A2, 2013 ;
