(4-氯苯基)(氧代)乙酰氯合成路线 （共 6 条）
反应条件
thionyl chloride in benzene 3 h; Heating;
参考文献
Sumitomo Chemical Company, Limited
Patent: EP1541557 A1, 2005 ;
Location in patent: Page/Page column 48 ;
反应条件
1: sodium hydroxide; water / 2 h / 20 °C 2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Enders, Dieter; Stoeckel, Bianca A.; Rembiak, Andreas
Chemical Communications, 2014 , vol. 50, # 34 p. 4489 - 4491
反应条件
1: KOH / H2O; ethanol 2: oxalyl chloride / CH2Cl2 / 0.5 h / cooling View Scheme
参考文献
Chen, Chien-Tien; Bettigeri, Sampada; Weng, Shiue-Shien; Pawar, Vijay D.; Lin, Ya-Hui; Liu, Cheng-Yuan; Lee, Way-Zen
Journal of Organic Chemistry, 2007 , vol. 72, # 22 p. 8175 - 8185
反应条件
1: VOCl3; O2 / acetonitrile 2: KOH / H2O; ethanol 3: oxalyl chloride / CH2Cl2 / 0.5 h / cooling View Scheme
参考文献
Chen, Chien-Tien; Bettigeri, Sampada; Weng, Shiue-Shien; Pawar, Vijay D.; Lin, Ya-Hui; Liu, Cheng-Yuan; Lee, Way-Zen
Journal of Organic Chemistry, 2007 , vol. 72, # 22 p. 8175 - 8185
反应条件
in toluene T=110°C; 3 h; Inert atmosphere;
参考文献
Kashiwabara, Taigo; Tanaka, Masato
Journal of Organic Chemistry, 2009 , vol. 74, # 10 p. 3958 - 3961
反应条件
1.1: triethylamine / dichloromethane / 0 - 20 °C
2.1: sodium hydride / tetrahydrofuran / 0 - 20 °C
2.2: 0 - 20 °C
3.1: [Ni0(1,5-cyclooctadiene)2]; dimethyl zinc; tri-cyclo-hexyl-phosphine / ethylene glycol dimethyl ether; toluene / 12 h / 40 °C / Inert atmosphere
View Scheme
参考文献
Hu, Jin-Xiu; Wu, Hao; Li, Chuan-Ying; Sheng, Wei-Jian; Jia, Yi-Xia; Gao, Jian-Rong
Chemistry - A European Journal, 2011 , vol. 17, # 19 p. 5234 - 5237
