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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1041479-70-2
合成路线
（共 7 条）
1041479-70-2
+
89523-62-6
→
反应条件
2050-68-2
4,4'-二氯联苯
+
14310-22-6
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=60°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
1041479-70-2
+
89523-62-6
→
反应条件
14310-22-6
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; 2-chloro-1,2-diphenyl-ethanone in tetrahydrofuran T=60°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
1041479-70-2
+
130447-21-1
→
反应条件
92-86-4
4,4-二溴联苯
+
14310-24-8
4-溴联苄基
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=20°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
67-56-1
甲醇
+
1041479-70-2
+
201230-82-2
→
反应条件
103-25-3
3-苯丙酸甲酯
反应条件
(+/-)-SynPhos; dichloro bis(acetonitrile) palladium(II); 2-chloro-1,2-diphenyl-ethanone T=60°C; P=7757.43 Torr; 24 h;
参考文献
Zhao, Yingsheng; Jin, Liqun; Li, Peng; Lei, Aiwen
Journal of the American Chemical Society, 2008 , vol. 130, # 29 p. 9429 - 9433
1041479-70-2
+
89523-62-6
→
反应条件
2050-68-2
4,4'-二氯联苯
+
14310-22-6
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=60°C; 5 h; chemoselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 351, # 4 p. 630 - 634
1041479-70-2
→
反应条件
6161-50-8
3,3-二甲氧基联苯
+
70610-09-2
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=60°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
1041479-70-2
+
130447-21-1
→
反应条件
92-86-4
4,4-二溴联苯
+
14310-24-8
4-溴联苄基
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=20°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
