乙酸-(4-苯基)-2-丁酯合成路线 (共 28 条)
反应条件
indium trifluoromethanesulfonate T=80°C; retro-Claisen condensation; 24 h;
参考文献
Kawata, Atsushi; Takata, Kazumi; Kuninobu, Yoichiro; Takai, Kazuhiko
Angewandte Chemie - International Edition, 2007 , vol. 46, # 41 p. 7793 - 7795
反应条件
pyridine 5 h; Ambient temperature;
参考文献
Ferraboschi, Patrizia; Grisenti, Paride; Manzocchi, Ada; Santaniello, Enzo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 9 p. 2469 - 2474
反应条件
tin(II) trifluoromethanesulfonate; p-trifluoromethylthiobenzoic anhydride in dichloromethane 3 h; Ambient temperature;
参考文献
Mukaiyama, Teruaki; Shiina, Isamu; Miyashita, Mitsutomo
Chemistry Letters, 1992 , # 4 p. 625 - 628
反应条件
in 1,2-dichloro-ethane T=20°C; 1 h;
参考文献
Kobayashi, Kumiko; Watahiki, Tsutomu; Oriyama, Takeshi
Synthesis, 2003 , # 4 p. 484 - 486
反应条件
sodium tetrahydroborate; nickel dichloride in methanol 0.333333 h; Ambient temperature;
参考文献
He, Yun; Pan, Xinfu; Zhao, He; Wang, Shaofei
Synthetic Communications, 1989 , vol. 19, # 17 p. 3051 - 3054
反应条件
N,N,N',N,-tetramethylethylenediamine; 4 A molecular sieve in dichloromethane T=-78°C; Acylation; 6 h;
参考文献
Sano; Ohashi; Oriyama
Synthesis, 1999 , # 7 p. 1141 - 1144
反应条件
1: (E)-4-phenyl-3-buten-2-one With [{(Ph3P)CuH}6]; hydrogen; (dimethyl)(phenyl)phosphine in tert-butyl alcohol; benzene T=20°C; Hydrogenation; P=25857.4 Torr; 18 h; 2: acetic anhydride With pyridine in tert-butyl alcohol; benzene T=0 - 20°C; Acetylation; Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 56, # 15 p. 2153 - 2166
反应条件
pyridine in dichloromethane 6 h; Ambient temperature; Yield given;
参考文献
Bateson, John H.; Quinn, Alison M.; Smale, Terence C.; Southgate, Robert
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 2219 - 2234
反应条件
[Zn(BH4)2(nmi)] in tetrahydrofuran 1 h; Reflux;
参考文献
Setamdideh, Davood; Khezri, Behrooz
Asian Journal of Chemistry, 2010 , vol. 22, # 7 p. 5766 - 5772