N,O-双三甲硅基乙酰胺合成路线 （共 163 条）
反应条件
Ambient temperature;
参考文献
Barton, Derek H. R.; Chern, Ching-Yuh; Jaszberenyi, Joseph Cs.
Tetrahedron, 1995 , vol. 51, # 7 p. 1867 - 1886
反应条件
tin(IV) chloride
1.) CH3CN, 80 deg C, 30 min; 2.) CH3CN, r.t.; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Janardhanam, Selvasekaran; Nambiar, Krishnan P.
Tetrahedron Letters, 1994 , vol. 35, # 22 p. 3657 - 3660
反应条件
potassium hydride
1.) THF, 1 h, 0 deg C, 2.) 70 h, RT; Yield given. Multistep reaction;
参考文献
Hwu, Jih Ru; Anderson, Denise A.; Wang, Naelong; Buchner, Meredith M.; Gani, Paul; Tsay, Shwu-Chen
Chemische Berichte, 1990 , vol. 123, # 8 p. 1667 - 1671
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide
Ambient temperature;
参考文献
Dedier, James; Gerval, Pierre; Frainnet, Emile
Journal of Organometallic Chemistry, 1980 , vol. 185, # 2 p. 183 - 198
反应条件
tetrabutylammomium bromide
T=105°C; 4 h;
参考文献
Smietana, Michael; Mioskowski, Charles
Organic Letters, 2001 , vol. 3, # 7 p. 1037 - 1039
参考文献
White,E. et al.
Journal of Organic Chemistry, 1970 , vol. 35, p. 4241 - 4244
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=40 - 50°C;
参考文献
Dedier, James; Gerval, Pierre; Frainnet, Emile
Journal of Organometallic Chemistry, 1980 , vol. 185, # 2 p. 183 - 198
参考文献
Piperno, Anna; Giofre, Salvatore V.; Iannazzo, Daniela; Romeo, Roberto; Romeo, Giovanni; Chiacchio, Ugo; Rescifina, Antonio; Piotrowska, Dorota G.
Journal of Organic Chemistry, 2010 , vol. 75, # 9 p. 2798 - 2805
反应条件
in acetonitrile
T=20°C;
参考文献
Semaine, Wassila; Johar, Monika; Tyrrell, D. Lorne J.; Kumar, Rakesh; Agrawal
Journal of Medicinal Chemistry, 2006 , vol. 49, # 6 p. 2049 - 2054
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide
Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Dedier, James; Gerval, Pierre; Frainnet, Emile
Journal of Organometallic Chemistry, 1980 , vol. 185, # 2 p. 183 - 198
