N,O-双三甲硅基乙酰胺合成路线 (共 163 条)
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide
Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Dedier, James; Gerval, Pierre; Frainnet, Emile
Journal of Organometallic Chemistry, 1980 , vol. 185, # 2 p. 183 - 198
反应条件
in acetonitrile
Ambient temperature;
参考文献
Basnak; Sun; Coe; Walker
Nucleosides and Nucleotides, 1996 , vol. 15, # 1-3 p. 121 - 134
参考文献
Kowalski,J.; Lasocki,Z.
Journal of Organometallic Chemistry, 1976 , vol. 116, p. 75 - 82
反应条件
in acetonitrile
T=50°C; silylation; 0.166667 h;
参考文献
Maddaford, Adrian; Guyot, Thierry; Leese, David; Glen, Rebecca; Hart, James; Zhang, Xiurong; Fisher, Ray; Middleton, Donald S.; Doherty, Cheryl L.; Smith, Nick N.; Pryde, David C.; Sutton, Scott C.
Synlett, 2007 , # 20 p. 3149 - 3154
反应条件
in 1,2-dichloro-ethane
T=50°C; 0.5 h; Inert atmosphere;
参考文献
Li, Nan-Sheng; Piccirilli, Joseph A.
Chemical Communications, 2012 , vol. 48, # 70 p. 8754 - 8756
参考文献
Pudovik, M. A.; Kibarbina, L. K.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 3.2 p. 771 - 772,699 - 700
参考文献
Pudovik, M. A.; Kibardina, L. K.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 5.1 p. 1058 - 1063,960 - 964
反应条件
tetrabutylammomium bromide
T=105°C; 4 h;
参考文献
Smietana, Michael; Mioskowski, Charles
Organic Letters, 2001 , vol. 3, # 7 p. 1037 - 1039
反应条件
pyridine
T=80°C; 2 h;
参考文献
Takano, Ryo; Matsuo, Masayoshi; Kamei-Hayashi, Kaeko; Hara, Saburo; Hirase, Susumu
Bioscience, Biotechnology, and Biochemistry, 1992 , vol. 56, # 10 p. 1577 - 1580
反应条件
in acetonitrile
2 h; Ambient temperature;
参考文献
Kraus, George A.; Wu, Yusheng
Anales de Quimica, 1995 , vol. 91, # 5-6 p. 394 - 398