N,O-双三甲硅基乙酰胺合成路线 (共 163 条)
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran Ambient temperature;
参考文献
Johnson
Carbohydrate Research, 1992 , vol. 237, p. 313 - 318
参考文献
Boto, Alicia; Hernandez, Dacil; Hernandez, Rosendo
European Journal of Organic Chemistry, 2010 , # 20 p. 3847 - 3857
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 43, # 1 p. 142 - 143
反应条件
hydrogenchloride; ammonium chloride; copper monoiodide in tetrahydrofuran; 1,4-dioxane; hexane; water; acetonitrile
参考文献
Beecham Group Limited
Patent: US4312874 A1, 1982 ;
反应条件
in acetonitrile T=100°C; 2 h;
参考文献
Horibe; Oshita
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 1 p. 181 - 182
反应条件
pyridine T=20°C; 1 h;
参考文献
Krafczyk, Nicole; Glomb, Marcus A.
Journal of Agricultural and Food Chemistry, 2008 , vol. 56, # 9 p. 3368 - 3376
反应条件
tetrabutylammomium bromide T=105°C; 4 h; Title compound not separated from byproducts.;
参考文献
Smietana, Michael; Mioskowski, Charles
Organic Letters, 2001 , vol. 3, # 7 p. 1037 - 1039
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Dedier, James; Gerval, Pierre; Frainnet, Emile
Journal of Organometallic Chemistry, 1980 , vol. 185, # 2 p. 183 - 198
反应条件
tributylphosphine in dichloromethane-d2 T=35°C; 18 h;
参考文献
Vedejs, E.; Bennett, N. S.; Conn, L. M.; Diver, S. T.; Gingras, M.; et al.
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7286 - 7288
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide 0.0333333 h; Ambient temperature;
参考文献
Dedier, James; Gerval, Pierre; Frainnet, Emile
Journal of Organometallic Chemistry, 1980 , vol. 185, # 2 p. 183 - 198